- Paperback: 610 pages
- Publisher: John Wiley & Sons Canada, Ltd.; 2nd Completely Revised and Enlarged Edition edition (Aug 27 1998)
- Language: English
- ISBN-10: 3527295127
- ISBN-13: 978-3527295128
- Product Dimensions: 24.3 x 17.1 x 3.2 cm
- Shipping Weight: 1.2 Kg
- Average Customer Review: 4.0 out of 5 stars See all reviews (1 customer review)
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Amazon Bestsellers Rank:
#2,110,200 in Books (See Top 100 in Books)
- #36 in Books > Science > Chemistry > Spectroscopy > NMR
- See Complete Table of Contents
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Product Details |
Product Description
Review
"... an essential purchase for all NMR devotees ... honest, well focused and most adequately produced ... A wealth of information is clearly expressed and provided." -- The Analyst
"...Every self-respecting NMR laboratory should consider acquiring this book. Ideally a copy of BKB should be placed next to every spectrometer..." -- Angewandte Chemie 4th February 2000
"...It is hard to imagine an NMR spectrometer without a copy of this book nearby..." -- Trends in Analytical Chemistry, February 2000
"The methods described are representative of the most important pulse sequences in modern high-resolution NMR spectroscopy....Of great value are the listings of realistic values of pulse-sequence parameters for each experiment....supplies substantial and detailed information for actually performing these experiments. It is state of the art with respect to methods and applications, and provides a most welcome help for the working spectroscopists in the routine NMR laboratory." -- Colloid and Polymer Science
"...Every self-respecting NMR laboratory should consider acquiring this book. Ideally a copy of BKB should be placed next to every spectrometer..." -- Angewandte Chemie 4th February 2000
"...It is hard to imagine an NMR spectrometer without a copy of this book nearby..." -- Trends in Analytical Chemistry, February 2000
"The methods described are representative of the most important pulse sequences in modern high-resolution NMR spectroscopy....Of great value are the listings of realistic values of pulse-sequence parameters for each experiment....supplies substantial and detailed information for actually performing these experiments. It is state of the art with respect to methods and applications, and provides a most welcome help for the working spectroscopists in the routine NMR laboratory." -- Colloid and Polymer Science
Book Description
From reviews of "100 and More Basic NMR Experiments": "... an essential purchase for all NMR devotees ... honest, well focused and most adequately produced ... A wealth of information is clearly expressed and provided." -- The Analyst "The methods described are representative of the most important pulse sequences in modern high-resolution NMR spectroscopy....Of great value are the listings of realistic values of pulse-sequence parameters for each experiment....supplies substantial and detailed information for actually performing these experiments. It is state of the art with respect to methods and applications, and provides a most welcome help for the working spectroscopists in the routine NMR laboratory." -- Colloid and Polymer Science Nuclear magnetic resonance(NMR) spectroscopy is one of the most powerful analytical techniques used in chemistry and physics. The magnetic resonance imaging (MRI) technique used by medical personnel to diagnose disease and injuries is a well known type of NMR. This new, expanded edition of a highly-successful book shows how to make the most efficient use of NMR using practical, goal-oriented experiments. An ideal reference and training manual for the laboratory, this book is a must for every scientist working with NMR as well as for students preparing for their lab courses.
Inside This Book
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First Sentence
In most current NMR spectrometers the magnetic field is generated by a superconducting magnet (Fig. 1.1). Read the first page
Front Cover | Copyright | Table of Contents | Excerpt | Index | Back Cover
In most current NMR spectrometers the magnetic field is generated by a superconducting magnet (Fig. 1.1). Read the first page
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Browse Sample PagesConcordance
Front Cover | Copyright | Table of Contents | Excerpt | Index | Back Cover
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Most helpful customer reviews
4.0 out of 5 stars
As the title says, your basic NMR spectroscopy catelog.,
By A Customer
This review is from: 150 and More Basic NMR Experiments: A Practical Course, 2nd Completely Revised and Enlarged Edition (Paperback)
NMR spectroscopy is a powerful tool for chemists interested in structure, dynamics and function of molecular systems. The success of this technique has lead to a proliferation of experiments yielding a wealth of data about chemical structure ranging from small molecules to not-so-small proteins and beyond. The authors have compiled a core of NMR experiments that will serve a student new to the field or an old-hand who has forgotten the phase-cycle of a particular pulse sequence. The book is sectioned into 14 chapters with the 1st two being introductory ( What is a NMR spectrometer and why is it sitting away from everything else? or If I have radiation dampening do I need to get a mop?). The next 10 chapters take the reader from routine spectroscopy experiments to a variety of 1- and 2- dimensional liquid NMR experiments with and without magnetic field gradients. The last two chapters introduce the reader to some basic 3-dimensional liquid sequences and solids NMR spectroscopy. These two subjects could have been extended but I imagine we will see that in the next volume, 150 to 300 NMR experiments. There are 160 (according to my count) different experiments and measurements discussed and each is organized to familarize the experimenter with the purpose of the experiment, the procedure to perform it, and some expected results for the experiment. The authors have wisely included a readers observation area for each section. This allows the utility of the book to grow as the reader gains experience with each NMR method. This book should be in any NMR laboratory and would be an added help to any course using NMR spectroscopy. I know any undergraduate organic chemistry course should get an attendance boost from experiment 8.15 where the students would determine the alcohol content in polish vodka. (As a student I would have suggested a more hands on approach.) The final upshot is this is an great compendium and should be a staple in any NMR laboratory period.
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Most Helpful Customer Reviews on Amazon.com (beta) Amazon.com:
4.5 out of 5 stars (2 customer reviews) 3 of 3 people found the following review helpful
4.0 out of 5 stars
As the title says, your basic NMR spectroscopy catelog.,
By A Customer - Published on Amazon.com
This review is from: 150 and More Basic NMR Experiments: A Practical Course, 2nd Completely Revised and Enlarged Edition (Paperback)
NMR spectroscopy is a powerful tool for chemists interested in structure, dynamics and function of molecular systems. The success of this technique has lead to a proliferation of experiments yielding a wealth of data about chemical structure ranging from small molecules to not-so-small proteins and beyond. The authors have compiled a core of NMR experiments that will serve a student new to the field or an old-hand who has forgotten the phase-cycle of a particular pulse sequence. The book is sectioned into 14 chapters with the 1st two being introductory ( What is a NMR spectrometer and why is it sitting away from everything else? or If I have radiation dampening do I need to get a mop?). The next 10 chapters take the reader from routine spectroscopy experiments to a variety of 1- and 2- dimensional liquid NMR experiments with and without magnetic field gradients. The last two chapters introduce the reader to some basic 3-dimensional liquid sequences and solids NMR spectroscopy. These two subjects could have been extended but I imagine we will see that in the next volume, 150 to 300 NMR experiments. There are 160 (according to my count) different experiments and measurements discussed and each is organized to familarize the experimenter with the purpose of the experiment, the procedure to perform it, and some expected results for the experiment. The authors have wisely included a readers observation area for each section. This allows the utility of the book to grow as the reader gains experience with each NMR method. This book should be in any NMR laboratory and would be an added help to any course using NMR spectroscopy. I know any undergraduate organic chemistry course should get an attendance boost from experiment 8.15 where the students would determine the alcohol content in polish vodka. (As a student I would have suggested a more hands on approach.) The final upshot is this is an great compendium and should be a staple in any NMR laboratory period.
3 of 3 people found the following review helpful
5.0 out of 5 stars
a handbook for spectroscopists,
By terry wolowiec "longball8t" - Published on Amazon.com
This review is from: 100 And More Basic Nmr Experiments: A Practical Course (Paperback)
100 and more basic NMR experiments is an essential book for anyone working in an NMR lab, who occasionally has to do more than a repetitive basic 1D protocol. Braun et. al. cover everything from a brief introduction to a spectrometer, to calibrations and standard tests, right through homo and heteronuclear 1,2, and 3 dimentional nmr.Each experiment is set out with a schematic of the pulse program, phase cycling,and processing parameters, as well as literature citations and practical examples. It is particularily useful for users of Bruker spectrometers, as a lot of the nomenclature is identical to those of the Bruker instruments. People who have never done a heteronuclear 2D experiment could get an acceptable spectrum with very little other lterature. |
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